Multiresidue Analysis of Insecticides and Other Selected Environmental Contaminants in Poultry Manure by Gas Chromatography/Mass Spectrometry

Aznar Roca, Ramón and Albero, Beatriz and Sánchez Brunete, Consuelo and Miguel, Esther and Tadeo, José L. (2014). Multiresidue Analysis of Insecticides and Other Selected Environmental Contaminants in Poultry Manure by Gas Chromatography/Mass Spectrometry. "Journal of Aoac International", v. 97 (n. 4); pp. 978-986. ISSN 1060-3271. https://doi.org/10.5740/jaoacint.SGEAznar.

Description

Title: Multiresidue Analysis of Insecticides and Other Selected Environmental Contaminants in Poultry Manure by Gas Chromatography/Mass Spectrometry
Author/s:
  • Aznar Roca, Ramón
  • Albero, Beatriz
  • Sánchez Brunete, Consuelo
  • Miguel, Esther
  • Tadeo, José L.
Item Type: Article
Título de Revista/Publicación: Journal of Aoac International
Date: July 2014
Volume: 97
Subjects:
Faculty: E.T.S.I. Agrónomos (UPM) [antigua denominación]
Department: Otro
Creative Commons Licenses: Recognition - No derivative works - Non commercial

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Abstract

An analytical method was developed for the simultaneous determination in poultry manure of 41 organic contaminants belonging to different chemical classes: pesticides, polycyclic aromatic hydrocarbons, polychlorinated biphenyls, and polybrominated diphenyl ethers. Poultry manure was extracted with a modified QuEChERS method, and the extracts were analyzed by isotope dilution GC/MS. Recovery of these contaminants from samples spiked at levels ranging from 25 to 100 ng/g was satisfactory for all the compounds. The developed procedure provided LODs from 0.8 to 9.6 ng/g. The analysis of poultry manure samples collected on different farms confirmed the presence of some of the studied contaminants. Pyrethroids and polycyclic aromatic hydrocarbons were the main contaminants detected.

More information

Item ID: 40833
DC Identifier: http://oa.upm.es/40833/
OAI Identifier: oai:oa.upm.es:40833
DOI: 10.5740/jaoacint.SGEAznar
Official URL: http://aoac.publisher.ingentaconnect.com/contentone/aoac/jaoac/2014/00000097/00000004/art00003
Deposited by: Memoria Investigacion
Deposited on: 21 Jun 2016 15:13
Last Modified: 12 Jun 2019 11:55
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